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Department Structure and Dynamics of Energy Materials

Program of the 8th X-ray School

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8th X-ray school, 18. - 22.11.2024, 10 a.m. - 4:30 p.m.

MONDAY, 18.11.

(Kolloquiumsraum H132)

GENERAL INTRODUCTION I:

  • Fundamentals of crystallography
  • Fundamentals of X-ray diffraction

  • Introduction into X-ray CoreLab
  • Excercise: Pattern indexation by hand

TUESDAY, 19.11.

(DV 338)

GENERAL INTRODUCTION II:

  • Recap of fundamentals (Quiz)
  • Elements of X-ray powder pattern, peak shapes, measuring strategies

  • Excercise on simulating X-ray powder patterns

WEDNESDAY, 20.11.

(X-lab, DV 338)

HANDS-ON TRAINIG AND PATTERN ANALYSIS I:

  • Instrument introduction (optics, detectors, sample carriers, sample preparation, measuring)
  • Crystallographic databases: ICSD + ICDD-PDF
  • Phase analysis of XRD powder pattern using Bruker EVA software

THURSDAY, 21.11.

(X-lab, DV 338)

HANDS-ON TRAINIG AND PATTERN ANALYSIS II:

  • Grazing incidence XRD
  • Non-ambient X-ray diffraction 
  • Automatic indexation (parallel)

  • LeBail refinement using Fullprof suite

FRIDAY, 22.11.

(X-lab, DV 338)

HANDS-ON TRAINIG AND PATTERN ANALYSIS III:

  • Grazing incidence XRD 
  • Non-ambient X-ray diffraction 
  • Automatic indexation (parallel)

  • Science talk
  • Quiz + Closing
 

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